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Metal-catalyzed oligomerizations are important reactions concerning both their chemistry and practical applications. 12 ,36,37 Since the catalysts [(Ti(IV), Zr(IV), Ni(l), and Ni(lI) complexes] used in coordination polymerization can also be active in oligomerization, catalyst systems and mechanisms will be discussed in more detail in Section 13.2.4. A short discussion of oligomerization with emphasis on the most important processes of practical significance, however, is appropriate here. The first metal-catalyzed ethylene dimerization reaction was accidentally discovered by Ziegler and coworkers while studying ethylene oligomerization to long-chain cx-olefins in the presence of aluminum alkyls 8 They observed that nickel impurities from the reactor caused dimerization instead of oligomerization leading to the formation of I-butene. In fact, the growth reaction (i.e., oligomerization of ethylene) is followed by a displacement reaction by ethylene catalyzed by nickel resulting in the formation of an oligomer and regeneration of the aluminum alkyl. The aluminum-catalyzed chain growth step takes place through insertion into the C-AI bond via a nonsymmetric four-center transition state 9 Nickel,40,41 like almost all metal catalysts (e.g., Ti and Zr) used for alkene dimerization, effects the reaction by a three-step mechanism. 12 Initiation yields an organometallic intermediate via insertion of the alkene into the metal-hydrogen bond followed by propagation via insertion into the metal-carbon bond [Eq. (13.8)]. Intermediate 11 either reacts further by repeated insertion [Eq. (13.9)] or undergoes chain transfer to yield the product and regenerate the metal hydride catalyst through ~-hydrogen transfer [Eq. (13.10)]: upc internet pl Internet Kubíčkova 870/5, Brno | Dostupnost UPC - Dostupný internet
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I think UPC Cablecom uses traffic shaping to artificially reduce the upload speed .... but it's not my package (I had Internet 50, now Internet 100). As indicated (Section 5.2.5), successful acquisition of multiple FIDs depends upon the ability of a sample population of nuclei to recover steady state equilibrium between radio-frequency pulses. Recovery to equilibrium between pulses relies upon the two main relaxation processes mentioned above, namely spin lattice and spin spin relaxation (see Section 5.2.5). Spin lattice relaxation is associated with relaying spin energy to the surroundings by such mechanisms as through-space dipolar coupling (see Section 5.2.7). This same spin lattice relaxation is primarily responsible for the restoration of the bulk magnetisation vector, M, to its original magnitude and position along the z-axis. The component of the bulk magnetisation vector as it recovers with time along the z-axis is referred to as longitudinal magnetisation or polarisation, Mz (t). Mz (t) obeys the following proportionality: Mz (t) 1 exp( t/T1 ) (5.14) =COUNTIF(A1, A )=1 This gives the particular solution y 1 25 [ ] 5 25 [ 1 1 [3] [4] [5] [6] If iMovie starts behaving unstably, you may need to trash your iMovie preferences and repair permissions on your Mac s hard disk. Follow these steps: oferte abonament internet upc Experiența Wi-fi La Tine Acasă Oferită De UPC | Komparatorul
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