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Figure 2.14 Alternative strategies for solid phase oligosaccharide synthesis. (a) Glycosyl donor immobilized by silyl ether linker to resin and activated for coupling by the anhydrosugar-thioglycoside coupling methodology (see Fig. 2.13). Final removal of the product is effected with uoride ions delivered from tetrabutyl ammmonium uoride (TBAF). (b) Glycosyl acceptor immobilized by thio-ether linker to resin aided by trimethylsilyl tri late (TMSOTf). Repetitive facile deprotection of benzoyl (Bz) protecting groups (sodium methoxide, NaOMe) and further TMSOTf assisted coupling of glycosyl donors to acceptors leads to the nal product that is removed from the resin by DTBP activation assisted by N-bromosuccinimide (NBS). Solid phase oligosaccharide synthesis is an excellent approach for the synthesis of combinatorial libraries of small oligosaccharides for use in screening in biological research. For most indicated protecting groups, see Fig 2.13, Trichloroethyloxycarbonyl (Troc) is another important protecting group in oligo-/polysaccharide synthesis. word aflame upc UPC - A | Office File API | DevExpress Help
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